Home / Products / (Z)-1-[4-(2-Chloroethoxy)phenyl]-1,2-diphenylbut-1-ene
CAS 97818-83-2 Tamoxifen Intermediate Tamoxifen Intermediate High Purity GMP Grade

(Z)-1-[4-(2-Chloroethoxy)phenyl]-1,2-diphenylbut-1-ene

IUPAC: (Z)-Chlorolefin View on PubChem
CAS NUMBER
97818-83-2
MOL. FORMULA
C24H23ClO
MOL. WEIGHT
362.90 g/mol
Scientific Overview

The compound's defining feature is its (Z)-configured tetrasubstituted alkene, which must be precisely controlled during synthesis to ensure the correct geometric isomer carries through to the final drug substance --- geometric isomer purity is pharmacologically critical, since the (Z)- and (E)-isomers of triphenylethylene SERMs display markedly different estrogen receptor binding profiles (tamoxifen is the Z-isomer; the E-isomer is a distinct, less desirable compound). The terminal chloroethyl group serves as the electrophilic handle for the subsequent amination step that installs the dimethylaminoethoxy side chain defining tamoxifen's final structure.

(Z)-1-[4-(2-Chloroethoxy)phenyl]-1,2-diphenylbut-1-ene, commonly known as "(Z)-Chlorolefin," is a stereodefined triarylbutene bearing a reactive chloroethoxy side chain. It is a critical late-stage intermediate in the industrial synthesis of tamoxifen and related triphenylethylene-based selective estrogen receptor modulators (SERMs) used in breast cancer therapy.

Full Technical Data
Chemical Name (Z)-1-[4-(2-Chloroethoxy)phenyl]-1,2-diphenylbut-1-ene ((Z)-Chlorolefin)
CAS Number 97818-83-2
IUPAC Name (Z)-Chlorolefin
Molecular Formula C24H23ClO
Molecular Weight 362.90 g/mol g/mol
Reaction Scheme
(Z)-1,2-Diphenyl-1-(4-hydroxyphenyl)-1-butene
NA
NA
(Z)-1-[4-(2-Chloroethoxy)phenyl]-1,2-diphenylbut-1-ene
NA
Commercial Applications

Tamoxifen API Manufacturing

Direct penultimate synthetic intermediate for tamoxifen, a first-line SERM used in hormone receptor-positive breast cancer treatment and prevention.

SERM Derivative Synthesis

Building block for structurally related triphenylethylene SERM analogs and research compounds.

Process Chemistry & Route Optimization

Used in API process development to establish stereoselective synthesis routes ensuring Z-isomer geometric purity.

Analytical Reference Standard

Supports HPLC/chiral method development for monitoring geometric isomer purity in tamoxifen manufacturing.

Market Therapeutic Focus
TAMOXIFEN INTERMEDIATE PHARMACEUTICAL MANUFACTURING ONCOLOGY / HORMONE-RECEPTOR THERAPEUTICS API PROCESS CHEMISTRY ANALYTICAL REFERENCE STANDARDS CRO/CDMO
Scientific Literature

Synthesis and Antiestrogenic Activity of Tamoxifen and Related Triarylethylenes

Authors: Jordan, V.C.

Br. J. Pharmacol.

Stereoselective Synthesis Routes for Tamoxifen Manufacturing

Authors: Coe, P.L. et al.

J. Chem. Soc. Perkin Trans. 1

Geometric Isomerism and Estrogen Receptor Binding of Triphenylethylene SERMs

Authors: Robertson, D.W. et al.

J. Med. Chem.

Peer Queries & FAQs
Why is the Z-configuration critical for this intermediate?
The geometric isomer carries through the final synthetic step to tamoxifen; since tamoxifen's pharmacological activity as an estrogen receptor antagonist depends on its Z-configuration, strict isomeric control at this stage is essential for API quality.
What is the final synthetic step from this intermediate to tamoxifen?
Nucleophilic displacement of the terminal chloride with dimethylamine installs the dimethylaminoethoxy side chain that defines tamoxifen's complete structure.
How is geometric purity monitored during manufacturing?
Via HPLC methods capable of resolving Z/E isomer ratios, ensuring the desired stereochemistry is maintained through to the final API.
What is the recommended storage condition?
Store in a tightly sealed container, protected from light and moisture, at room temperature or as specified by supplier-specific stability data.

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